| COLS. INDEPENDENCE Seed: 9 3 |
| Date: 5/6/2024 Time: 6:00 PM |
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25-16, 25-17, 25-18
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| COLS. SOUTH Seed: 10 0 |
| WILLIAMSPORT WESTFALL Seed: 5 0 |
| Date: 5/7/2024 Time: 6:00 PM |
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25-20, 25-16, 25-23
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| COLS. BISHOP HARTLEY Seed: 6 3 |
| CHILLICOTHE Seed: 2 3 |
| Date: 5/7/2024 Time: 6:00 PM |
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25-11, 25-10, 25-9
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| COL. PATRIOT PREPARATORY Seed: 11 0 |
| COLS. ST. CHARLES Seed: 1 3 |
| Date: 5/9/2024 Time: 6:00 PM |
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25-7, 25-8, 25-7
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| COLS. INDEPENDENCE Seed: 9 0 |
| EAST DAYTON CHRISTIAN Seed: 7 0 |
| Date: 5/9/2024 Time: 6:00 PM |
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25-12, 25-9, 25-19
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| COLS. BISHOP HARTLEY Seed: 6 3 |
| COLS. BISHOP WATTERSON Seed: 3 3 |
| Date: 5/9/2024 Time: 6:00 PM |
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25-20, 25-20, 25-17
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| DAYTON ARCHBISHOP CARROLL Seed: 8 0 |
| COLS. ST. FRANCIS DeSALES Seed: 4 3 |
| Date: 5/9/2024 Time: 6:00 PM |
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25-19, 26-24, 25-20
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| CHILLICOTHE Seed: 2 0 |
| COLS. ST. CHARLES Seed: 1 3 |
| Date: 5/14/2024 Time: 6:00 PM |
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25-8, 25-7, 25-14
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| COLS. BISHOP HARTLEY Seed: 6 0 |
| COLS. BISHOP WATTERSON Seed: 3 2 |
| Date: 5/14/2024 Time: 6:00 PM |
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19-25, 25-19, 17-25, 25-21, 15-11
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| COLS. ST. FRANCIS DeSALES Seed: 4 3 |
| COLS. ST. CHARLES Seed: 1 3 |
| Date: 5/18/2024 Time: 3:00 PM |
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25-20, 25-16, 25-22
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| COLS. ST. FRANCIS DeSALES Seed: 4 0 |
| COLS. ST. CHARLES |
| Region 5 Winner | | Advances to Wittenberg University | | Saturday, May 25 | | 1:00 PM |
|
